Eutech Instruments Cyberscan PH 1100 2100 Phion Meter
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Documents

Deluxe Bench pH/Ion Meter
CyberScan pH 1100 Meter
pH / mV (ORP) / oC / oF / RS 232
CyberScan pH 2100 Meter
pH / Ion / mV (ORP) / oC / oF / RS 232
Large Bright, Backlit, Dot Matrix Display Microprocessor Based 0.01 / 0.002 pH Accuracy - Selectable Multi-point Calibration with Auto-buffer Recognition Choice of USA, NIST or User-definable buffer standards 100 Memory Data Sets with Date/Time Stamping, GLP compliant Audible Limit Alarm and Auto Datalogging Electrode Diagnosis RS232C, Recorder Output
Technology Made Easy.
Splash-proof Keypad
Large character dot-matrix LCD with date/time display
Back Panel
Slide-out Instruction Card
Designed for optimum power, versatility, and ease of use in your lab the CyberScan pH2100 Series uses one of the latest Application Specific Integrated Circuit (ASIC) technologies. Sophisticated and advanced in features, these meters are still easy to use.
MULTI-PARAMETER MEASUREMENT The research-grade microprocessor-based CyberScan pH 1100/2100 measures direct Ion concentration (for pH 2100), pH, mV (ORP) and temperature (oC/oF) fast, accurately and easily. MULTI-POINT PUSH BUTTON CALIBRATION WITH CAL DUE PROMPT Up to 5-point pH calibration improves accuracy. Choice of USA, NIST or mix and match buffers meets changing laboratory needs. Auto buffer recognition simplifies calibration process. 5-point Ion calibration ensures good accuracy across full ion measurement range. CAL Due prompts you when next calibration is due. AUTOMATIC TEMPERATURE COMPENSATION Built-in Automatic Temperature Compensation (ATC) corrects readings inspite of changing sample temperatures. NON-VOLATILE MEMORY WITH DATE/TIME STAMPING Up to 100 data sets can be stored to memory. Data is time and date indexed; complies to Good Laboratory Practice (GLP) requirements. LIMIT ALARM SETTING Audible alarm alerts you when measurements exceed preset high or low set points. ELECTRODE DIAGNOSIS Electrode characteristics can be viewed via the setup menu to check electrode condition. DATA LOG/PRINT AND BI-DIRECTIONAL RS 232 COMMUNICATION Take control of the meter remotely using Data Acquisition Software (DAS) provided as a standard accessory. Log Data to memory or print at preset time intervals. Or data can be downloaded to any spreadsheet program on your PC via the DAS. An analogue recorder output allows linkup to an external chart recorder or recording device. LARGE BRIGHT-LIT DOT-MATRIX DISPLAY High contrast, backlit, large character dot matrix LCD (Liquid Crystal Display) gives you a clear view. Self-diagnostic message codes helps you keep your meter in good working condition. AESTHETIC DESIGN A slide-out instruction card serves as a handy reference guide for keypad functions and troubleshooting. Splash-proof keypad protects the meter from accidental spills. Audible tactile feedback confirms key selection. Anti-skid footpads prevent meter from sliding on bench-tops. WARRANTY Eutech Instruments supplies these meters with 3-year warranty against manufacturing defects and 6-month warranty for electrodes.
Eutech Instruments also provides meter accessories, ISE and calibration standards. Refer to separate brochures for information. Note: Eutech Instruments reserves the right to make changes, improvements and modifications to products shown.
Specifications: CyberScan pH Ion Concentration Range (for pH2100 only) Resolution & accuracy pH Range Resolution & accuracy mV Range Resolution & accuracy Relative mV Range Resolution & accuracy Temperature Range Resolution & accuracy Temperature Compensation No. of ion calibration points No. of pH calibration points pH buffer options
1100 / pH 2100 0.001 to LSD & 0.5% of reading -1.000 to 14.000 pH 0.01/0.001 pH & 0.01/0.002 pH -1850 to +1850 mV 0.1 mV & 0.2 mV -1850 to +1850 mV 0.1 mV & 0.2 mV -5.0 to 105.0 oC (23.0 to 221.0 oF) 0.1 oC (0.1 oF) & 0.5 oC (0.9 oF) Automatic/Manual (0 to 100oC) 5 (min. 2 points) 1 to 5 USA: 1.68, 4.01, 7.00, 10.01, 12.45 NIST: 1.68, 4.01, 6.86, 9.18, 12.45 User 1: 1.68, 4.01, 7.00, 9.18, 12.45 User 2: 1.68, 4.01, 6.86, 10.01, 12.45 Custom: min. of 2 and max. of 5 points Yes 100 Data Sets (with date/time stamping) Alpha Numeric LCD (2 lines/20 characters) with backlight RS232C, Recorder ( 1850 mV) 0 to 50 oC Power adapter, 9V DC 500 mA output 120/220 VAC input Meter: 18 x 23 x 6 cm; 950g Boxed: 40 x 26 x 9 cm; 1650g
pH Slope and Offset Display Memory Display Output Operating Temperature Power requirements Dimension/Weight
ORDERING INFORMATION Order No. Item
EC-PH1100/01S EC-PH2100/01S EC-FG73504-01B EC-FC72522R-01B EC-PH5-TEMB01P 60X03111 60X03112 CyberScan pH1100 meter with EC-PH5-TEMB01P and integral electrode stand CyberScan pH 2100 meter with EC-PH5-TEMB01P and integral electrode stand Glass-body refillable pH combination electrode (1m cable) Plastic-body refillable double-junction pH combination electrode (1m cable) Temperature probe (1m cable) 110 VAC power adapter (50/60 Hz) 220 VAC power adapter (50/60 Hz)
Distributed By:
Eutech Instruments Pte Ltd
55, Ayer Rajah Crescent, #04-16/24, Singapore 139949 : (65) : (65) : marketing@eutechinst.com
e: http://www.eutechinst.com
Eutech Instruments Europe B.V.
P.O.Box 254, 3860 AG Nijkerk Netherlands : (31) 33-2463887 : (31) 33-2460832
: info@eutech.nl e: http://www.eutech.nl
BEN 08X233308 7/03 Rev 1

Instruction Manual
pH 1100/ pH 2100
Bench pH/Ion Meter
Technology Made Easy.
68X090818 rev 2.2 Nov 02
CyberScan pH 1100/ 2100
PREFACE
Thank you for selecting the pH 1100/ 2100 benchtop meter. This meter measure pH, millivolts, relative millivolts and temperature. The pH 2100 meter also measures ion concentration. The instruction manual serves to explain the use of the pH 1100/ 2100 bench meter as a step-by-step operational guide to help you familiarize with the meters features and functions. It is structured sequentially with illustration of diagrams that explains the various functions and setup menus available. This manual is written to cover as many anticipated applications and uses of the pH 1100/ 2100 Bench meter as possible. If there are doubts in the use of the meter, please do not hesitate to contact the nearest Authorized Distributor or Customer Service Dept. for assistance. Eutech Instruments/ Oakton Instruments reserve the rights to change, make improvement and modify specifications without prior notice and cannot accept any responsibility for damage or malfunction to the instrument caused by improper use.
Copyright 2002 Eutech Instruments Pte. Ltd. Oakton Instruments All rights reserved. Revision 2.2, Nov 02.
TABLE OF CONTENTS
1 INTRODUCTION 1.1 1.2 1.3 1.Introducing the Bench Meter Series Keypad Rear Panel Electrode Holder 35
STARTING UP 2.1 Back Panel Connections 2.2 Powering up and powering down 2.2.1 Powering up 2.2.2 Powering down
CALIBRATION & MEASUREMENT
3.1 pH calibration 3.1.1 Automatic Temperature Compensation (ATC) 3.1.2 Starting pH calibration 3.1.3 Standard pH buffer calibration 3.1.4 Custom pH buffer calibration 3.1.5 Calibration error messages 3.2 pH measurement 3.2.1 Automatic temperature compensation 3.2.2 Adjusting manual temperature compensation 3.2.3 Taking pH Measurements 4 mV CALIBRATION AND MEASUREMENT 4.1 mV Calibration 4.1.1 mV Calibration error message 4.2 mV Measurement 5 ION CALIBRATION AND MEASUREMENT (ONLY APPLICABLE FOR pH 2100) 5.1 5.2 5.Ion calibration Ion calibration error messages Ion measurement
MEMORY FUNCTIONS 6.1 Memory input 6.1.1 Manually storing a reading into memory 6.2 Memory recall 6.2.1 Recalling readings in manual recall mode 6.2.2 Recalling readings in automatic recall mode
STABILITY INDICATOR ALARM FUNCTIONS 8.1 8.2 High and Low measurement alarm Calibration due alarm Temperature Calibration Temperature Calibration Error Messages
TEMPERATURE CALIBRATION 9.1 9.2
10 SETUP MODE 10.1 Setup mode overview 10.1.1 pH/Temperature setup submenus 10.1.2 mV setup submenus 10.1.3 Ion setup submenus (pH 2100 only) 10.1.4 Meter general configuration setup submenus 10.2 pH/ temperature setup mode 10.2.1 Entering pH/temperature setup mode 10.2.2 pH buffer setup program P1.0 10.2.3 pH resolution setup program P1.1 10.2.4 Temperature unit setup program P1.2 10.2.5 pH Measurement Alarm Setup Program P1.3 10.2.6 pH Calibration Due Alarm Setup program P1.4 10.2.7 Stability Setup Program P1.5 10.2.8 View pH calibration data setup program P1.6
10.2.9 pH calibration data reset setup program P1.7 10.3 mV setup mode 10.3.1 Entering mV setup mode 10.3.2 mV measurement alarm setup program P2.0 10.3.3 mV calibration due alarm setup program P2.1 10.3.4 Stability setup program P2.2 10.3.5 View mV calibration data setup program P2.3 10.3.6 mV calibration data reset setup program P2.4 10.4 Ion setup mode (pH 2100 meter only) 10.4.1 Entering ion setup mode 10.4.2 Ion unit setup mode P3.0 10.4.3 Ion measurement alarm setup program P3.1 10.4.4 Ion calibration due alarm setup program P3.2 10.4.5 Stability setup program P3.3 10.4.6 Ion mode setup program P3.4 10.4.7 View ion calibration data setup program P3.5 10.4.8 Ion calibration data reset setup program P3.6 10.5 Meter general configuration setup mode 10.5.1 Entering meter general setup mode 10.5.2 Date/time setup mode P4.0 10.5.3 Backlight setup mode P4.1 10.5.4 Data log setup mode P4.2 10.5.5 Memory recall setup mode P4.3 10.5.6 Communication setup mode P4.4 10.5.7 Data transfer setup mode P4.5 10.5.8 Memory clear setup mode P4.6 10.5.9 Meter reset setup mode P4.ELECTRODE CARE 11.1 11.2 11.3 Electrode Activation Electrode Maintenance Storing pH/ORP electrodes
Connector
ATC INPUT
Function
For phono jack connection from the temperature probe for Automatic Temperature Compensation. The probe should be a 30K thermistor probe. For connecting sensors with a BNC connector to the meter. The meter accepts any pH, ORP or ISE electrode with a BNC connector. Always make sure that the connector is clean and dry. For connection to the pin tip type reference electrode normally used with half cell (mono) type pH or ISE electrodes. For connection to the strip chart recorder. For connection to the ground earth jack (standard pin tip connectors). For connection to the RS232C serial port. For connection of the AC adapter power supply (included).
REF REC GND RS232 DC
Electrode Holder
The electrode holder is included in the same box as the meter.
To attach the electrode holder to the meter: 1. The electrode holder base attached to the bottom of the meter comes in the shipping position. See Figure 3. Use a Phillips screwdriver to remove the screw holding the electrode holder in shipping position. See Figure 3. Slide the electrode base away from the meter until the second screw slot lines up with the original screw hole. Use the screw removed earlier to secure electrode holder base into position. See Figure 3. The electrode holder arm is reversible. If desired, remove screw holding electrode holder base and slide base out of brackets. Slide base into brackets on opposite side and replace screw. To install the electrode arm, turn meter back to the upright position. See Figure 4. Line up the hole on the base of the electrode holder arm with the peg on the electrode holder base. Slide the hole securely onto the electrode holder base. See Figure 4. The electrode arm is now ready to swing into desired position.
Figure 3: Bottom of Meter
Figure 4: Fix electrode holder arm to holder base
STARTING UP
Attention: Do not get water on the BNC connector during operation. Avoid touching the connector with soiled or wet hands.
2.1 Back Panel Connections
Refer back to Figure 2. Make the necessary connections as mentioned in Section 1.3 Rear Panel, pg 8.
2.2.1 1.
Powering up and powering down
3.1.3 1.
Standard pH buffer calibration
When entering the standard calibration mode, the first buffer calibration point for standard pH buffers is 7.000 or 6.860 (depending upon which pH buffer set is selected). The upper display shows the current reading, the lower display will show Auto Buf Scan: 7.000 (or 6.860). The upper display will flash pH until the reading has stabilized. See Figure 16. If the selected buffer value is not within 1.0 of the measured pH value, the Auto pH Scan will continue to change until the pH buffer is within 1.0. When pH reading has stabilized, press ENTER. The lower display flashes *pH Offset Cal Done. See Figure 17. This calibration point is now stored in the meter. If you are performing a one-point calibration, press EXIT. The screen flashes Sys Updating.Please wait.The meter then returns to the pH measurement mode. You may now start taking pH readings. If you are performing a multi-point calibration, go to step 3.
7.001pH 25.4C ATC Auto Buf Scan: 7.000
Figure 16
7.001pH 25.4C ATC *pH Offset Cal Done
Figure 17
ATC 10.010pH 25.4C 2 Point Cal Done *
Figure 18
Rinse the probe with deionized water or a rinse solution, and place it in the next pH buffer. The lower display automatically scans to the next pH buffer solution. Wait for the measured pH value to stabilize. The upper display will flash pH until the reading has stabilized. When pH reading has stabilized, press ENTER. The lower display flashes 2 Point Cal Done * (3 if you have calibrated 3 points,4 if 4 points, etc.). See Figure 18. This calibration point is now stored in the meter. Repeat steps 3-5 for each point you wish to calibrate. When you are finished calibrating, press EXIT. The screen flashes Sys. Updating. Please wait. The meter then returns to the pH measurement mode. You may now start taking pH readings. If you perform a complete 5-point pH calibration, when you calibrate the fifth point and press ENTER, the meter automatically returns to measurement mode. You may now start taking pH readings.
Error: Cal Aborted
Figure 45
The meter is now in Rel mV measurement mode. See Figure 46. If you have not performed a mV calibration or have reset the meter, the display will read Abs. mV. See Figure 47. 2. Dip the electrode into the sample. The sensor or glass bulb of the electrode must be completely immersed into the sample. Stir the electrode gently to create a homogeneous sample. Allow time for the reading to stabilize. The upper display will show the mV reading, and the lower display will show the current month, day and time. See Figure 46.
Figure 46
Figure 47
ION CALIBRATION AND MEASUREMENT (ONLY APPLICABLE FOR pH 2100)
The pH 2100 meter reads ion concentration in ppm, ppt, mg/l, g/l, mmol/l and mol/l units. See Ion setup Program P3.0 (page 43) to select ion concentration units.
Ion calibration
This instrument is capable of up to 5-point custom ion calibration with a minimum of 2-point calibration. Custom calibration values can be any value between 0.001 and 19998. Once the first calibration value is keyed in, all other calibration will automatically be at least one decade apart. For example if your first calibration point is at 0.001, all other calibration points will be at least one decade apart from 0.001 (0.001, 0.01, 0.1,1.0, 10.0, 100, 1000, 10000). For best accuracy calibrate your meter to points with similar concentrations to the solutions you want to test. 1. 2. Connect an Ion Selective Electrode (ISE) to the BNC input connector on the back of the meter. Turn the meter ON. If the meter is not in the Ion measurement mode, press EXIT and use >/CAL to select Ion. The mode selected will flash. See Figure 48. Press ENTER to confirm selection. The meter is now in Ion measurement mode. If the meter has not been calibrated or has been reset, the display will flash Ion Meas and current mV value. See Figure 49. If the meter has been calibrated previously, the display will show the current concentration value plus the absolute mV produced by the electrode. Dip the electrode into the first calibration standard. Start with the calibration standard that has the lowest concentration and move up to higher concentration standards. Press >/CAL to enter the ion calibration mode. The display will flash Cal Mode Activated, Please wait. See Figure 50. The display then shows Ion Conc: ppm (or unit selected in ion setup mode) in the upper display and Abs. mV: in the lower display. See Figure 51. The first calibration point must be keyed in by the user. Key in the concentration value of the standard using the numeric keypad. If you make a mistake, use the /MI or /MR keys to highlight mistake, then re-enter. Press ENTER to confirm the first calibration point. The display will flash 1 Cal Point Done *, then the meter proceeds to the next calibration point at least 1 decade apart from the first calibration point. See Figure 52. Use /MI or /MR keys to move the cursor to next calibration point. All points will be a decade apart from the first calibration point. Rinse off the electrode with deionized water before placing it in the next calibration standard.
Ion calibration error messages
If you leave the ion calibration mode prior to confirming two calibration points by pressing the EXIT key, the screen will flash Error: Cal Aborted. See Figure 56. The meter will revert to back to the earlier calibration curve and return to the ion measurement mode. If the average ion slope is not within 10 to 75 mV per decade, the upper display will flash Error: and the lower display will read Ion Slope Error. See Figure 57.
Figure 56
Error : Ion Slope Error
Figure 57
Ion measurement
The pH 2100 meter features two different modes of ion measurement: high resolution mode and low resolution mode. These modes are user selectable in the Ion setup program P3.4. (page 47). The default is high resolution mode. Low resolution mode should only be used if your ion solution concentration will produce an absolute mV value of 500 mV. 1. Turn the meter ON. If the meter is NOT in the Ion measurement mode, press EXIT and use >/CAL to select Ion. The mode selected will flash. See Figure 58. Press ENTER to confirm selection. The meter is now in Ion measurement mode. If the meter has not been calibrated, or has been reset, the display will flash Ion Meas and current mV value. See Figure 59. If the meter has been calibrated, the display will show the current concentration value plus the absolute mV produced by the electrode. See Figure 60. Prepare samples as necessary. Sample preparations varies depending on ion typesee your electrode manual for details on the specific electrode that you are using. Dip electrode into the sample. The sensor or glass bulb of the electrode must be completely immersed into the sample. Allow time for the reading to stabilize, then record your measurement.
Figure 58
Figure 59
0.013ppm 160.3mV Jan 21:35:34
Figure 60
NOTE: The display in the ion measurement mode shows mV that correlates to the electrode output. Charge in mV will typically be 59.7 mV for monovalent ions (1+ or 1- charge) and 29.8 mV for divalent ions (2+ or 2- charge).
MEMORY FUNCTIONS
Memory input
This meter can store up to 100 sets of data in several combinations: pH 1100 meter: pH, temperature, date and time mV, temperature, date and time pH 2100 meter: pH, temperature, date and time mV, temperature, date and time ion, mV, date and time For example, you can store 32 pH and 68 mV values for the pH 1100 or 50 ion, 25 mV and 25 pH values for the pH 2100. This meter can be setup to log readings automatically or manually. To set the meter to log automatically, see Meter Setup Program P4.2, Data Log Setup (page 52). The meter can log readings at intervals from 10 seconds to 23 hours 59 minutes and 59 seconds. 6.1.1 1. 2. Manually storing a reading into memory
Setup Mode Activated Please wait.
Figure 79
Setup: pH/Temp Meter Select & Press ENTER
Figure 80
pH Buffer Setup:P1.0 Press ENT. to Select
Figure 81
10.2.2
pH buffer setup program P1.0
Use this program to select calibration buffer sets: USA, NIST, Bf1, Bf2 or custom. Selectable buffer sets: USA: 1.68, 4.01, 7.00, 10.01, 12.45 NIST: 1.68, 4.01, 6.86, 9.18, 12.45 Bf1: 1.68, 4.01, 7.01, 9.18, 12.45 Bf2: 1.68, 4.01, 6.86, 10.01, 12.45 Custom: any 5 user selected custom buffers 1. Enter the pH/Temperature setup mode as described above (10.2.1 Entering pH/temperature setup mode). The first setup mode is pH Buffer Setup: P1.0. See Figure 81. Press ENTER to enter program pH Buffer Setup: P1.0. Press >/CAL key to toggle between USA NST Bf1 Bf2 Cust. Buffer set selected will flash. See Figure 82. Press ENTER to confirm selection and return to the setup mode. Press /MI key to continue to the next setup program, or press /MR to go to the previous program (P1.7 pH Calibration Reset). Press EXIT to return to the pH measurement mode.
USA NST Bf1 Bf2 Cust Select & Press ENTER
Figure 82
10.2.3
pH resolution setup program P1.1
Use this program to select pH resolution (0.01 or 0.001 pH). 1. 2. 3. 4. 5. Enter pH/Temperature setup mode as described in steps 1-4 in 10.2.1 Entering pH/temperature setup mode (page 30). Use /MI key to scroll to program pH Resol. Setup: P1.1. See Figure 83. Press ENTER to enter program pH Resol. Setup: P1.1. Press >/CAL to toggle between 0.01 and 0.001. The resolution selected will flash. See Figure 84. Press ENTER to confirm selection and return to the setup mode. Press /MI to continue to the next setup program, or press /MR to go to the previous program. Press EXIT to return to the pH measurement mode.
Figure 83
0.01 0.001 Select & Press ENTER
Figure 84
Figure 85
10.2.4
Temperature unit setup program P1.2
Use this program to select temperature measurement unit (C or F). 1. 2. 3. 4. 5. Enter pH/Temperature setup mode as described in steps 1-4 in 10.2.1 Entering pH/temperature setup mode (page 30). Use /MI key to scroll to program Temp Unit Setup: P1.2. See Figure 85. Press ENTER to enter program Temp Unit Setup: P1.2. Press >/CAL to toggle between Degree C and Degree F. The unit selected will flash. See Figure 86. Press ENTER to confirm selection and return to the setup mode. Press /MI to continue to the next setup program, or press /MR to go to the previous program. Press EXIT to return to the pH measurement mode.
Degree C Degree F Select & Press ENTER
Figure 86
10.2.5
pH Measurement Alarm Setup Program P1.3
7. Press ENTER to confirm number of days to next calibration,
10.2.7
Stability Setup Program P1.5
Use this program to turn on or off the pH stability indicator and to set level of stability (low, medium or high). Stability definitions High stability: reading is stabilized quickly, but reading is less accurate. Medium stability: reading stability is averaged between high and low stability. Low stability: reading is stabilized slowly, but guarantees high accuracy 1. 2. 3. 4. 5. Enter pH/Temperature setup mode as described in steps 14 in 10.2.1 Entering pH/temperature setup mode (page 30). Use /MI to scroll to program Stability Setup: P1.5. See Figure 94. Press ENTER to enter program Stability Setup: P1.5. Press >/CAL key to toggle between pH Stable Criteria: On and Off. The selection will flash. See Figure 95. Press ENTER to confirm selection. If you selected On, continue to step 6. If you select Off, pressing ENTER returns to the setup mode.
Stability Setup : P1.5 Press ENT. to Select
Figure 94
pH Stable Criteria On Off
Figure 95
Degree of Stability Low Medium High
Figure 96
Press /MI to continue to the next setup program, or press /MR to go to the previous program. Press EXIT to return to the pH measurement mode. 6. If you selected On in step 5, the display now reads Degree of Stability: Low Medium High. Press >/CAL to toggle between Low, Medium and High. The selection will flash. See Figure 96.
Press ENTER to confirm selection and return to the setup mode. Press /MI to continue to the next setup program, or press /MR to go to the previous program. Press EXIT to return to the pH measurement mode. Mode
10.2.8
View pH calibration data setup program P1.6
Use this program to view the following: Last pH calibration date/time pH buffer set selected pH calibration temperature and temperature compensation pH offset value pH slopes (from acid to alkaline) 1. 2. 3. Enter pH/Temperature setup mode as described in steps 1-4 in 10.2.1 Entering pH/temperature setup mode (page 30). Use /MI to scroll to program pH Cal Data: P1.6. See Figure 97. Press ENTER to enter program pH Cal Data: P1.6. The first screen in pH Cal Data: P1.6 is the pH Cal Date/Time. See Figure 98. Press ENTER to proceed to the second screen. This screen shows current buffer set and calibration points. See Figure 99. Press ENTER to proceed to the third screen. This screen shows calibration temperature and temperature compensation mode. See Figure 100. Press ENTER to proceed to the fourth screen. This screen shows current pH offset value in mV. See Figure 101. Press ENTER to proceed to the fifth screen. This screen shows current acid slope 1 and 2. See Figure 102. Press ENTER to proceed to the sixth screen. This screen shows current acid slope 2 and alkaline slope 1.See Figure 103. Press ENTER to proceed to the seventh screen. This screen shows current alkaline slope 1 and 2.See Figure 104.
Figure 155
Ion Reset: Yes No Select & Press ENTER
Figure 156
Ion being Reset Please wait.
Figure 157
Figure 158
This is the last ion setup program. Press /MR to go to the previous program. Press /MI to go back to the first ion setup program. Press EXIT to return to mV measurement mode. Mode
10.5 Meter general configuration setup mode
10.5.1 1. Entering meter general setup mode
Turn the meter ON. The meter setup mode can be entered from any measurement modepH, mV or ion (pH 2100 meter only). Press SETUP to enter the setup mode. The display will flash Setup Mode Activated, Please wait.See Figure 159. Use >/CAL to select "Meter". The mode selected will flash. See Figure 160, 161 and 162. Press ENTER to enter Meter setup mode. You are now in the Meter setup mode. The first setup program in Ion mode is Date/Time Setup: P4.0. See Figure 163. If you want to skip to another program, use the /MI and /MR keys to scroll to the desired program. To exit the setup mode at anytime, press EXIT. The meter returns to the measurement mode that it was in prior to entering meter setup mode.
Figure 159
Setup:pH/Temp Meter Select & Press ENTER
Figure 160
Figure 161
Figure 162
10.5.2
Date/time setup mode P4.0
Use this program to set the meter date and time. 1. Enter the Meter setup mode as described above in Section 10.5.1 Entering meter general setup mode (Pg 50). The first setup mode is Date/Time Setup: P4.0. See Figure 163. Press ENTER to enter program Date/Time Setup: P4.0. Key in the Date, Month, Year, Hr and Min using the numeric keypad. Use the >/CAL key or the ENTER key to toggle to each field. If you make a mistake keying the value, use the /MI and /MR keys to highlight mistake, then re-enter. See Figure 164. After keying in a value for the last field (Min), press ENTER to confirm. The screen flashes Clock Updating, Please wait. See Figure 165. The clock then flashes the date and time. See Figure 166. Press /MI key to continue to the next setup program, or press /MR to go to the previous program. Press EXIT to return to the measurement mode you were in prior to entering meter setup mode.
Figure 163
Date:23 Month:01 Year:02 Hr:8 Min:07
Figure 164
Clock Updating Please wait.
Figure 165
Date Time Jan 0807:31
Figure 166
10.5.3
Backlight setup mode P4.1
Use this program to turn backlight on or off and set duration time (0.1 to 10 minutes). 1. 2. 3. 4. 5. Enter meter setup mode as described in steps 1-4 in Section 10.5.1 Entering meter setup mode (page 50). Use /MI key to scroll to program Backlight Setup: P4.1. See Figure 167. Press ENTER to enter program Backlight Setup: P4.1. Press >/CAL key to toggle between Backlight On and Off. The selection will flash. See Figure 168. Press ENTER to confirm selection. If you selected On, continue to step 6. If you select Off, pressing ENTER returns to the setup mode.
Mem Clear Setup :P4.6 Press ENT. to Select
Figure 181
Memory Clear:Yes No Select & Press ENTER
Figure 182
Memory being Cleared Please wait.
Figure 183
10.5.9
Meter reset setup mode P4.7
Resets the meter to factory default settings: pH/mV/Ion* calibration data is erased Manual temperature compensation is set to 25.0C pH/mV/Ion* measurement alarm is off pH/mV/Ion* calibration due alarm is off Stability indicator is turned on with low stability setting Data logging and memory recall has manual setting Backlight is on with 2.0 minute duration Memory is cleared *Ion features on the CyberScan pH2100 meter only 1. 2. 3. 4. 5. Enter meter setup mode as described in steps 1-4 in Section 10.5.1 Entering meter setup mode (page 50). Use /MI key to scroll to program Meter Reset: P4.7. See Figure 184. Press ENTER to enter program Meter Reset: P4.7. Press >/CAL key to toggle between Meter Reset Yes and No. The selection will flash. See Figure 185. Press ENTER to confirm selection. If you selected Yes, the screen flashes Meter being Reset, Please wait.See Figure 186. The meter then returns to measurement mode. If you select No, the screen flashes Reset Aborted. See Figure 187. The meter then returns to the measurement mode.
Figure 184
Meter Reset: Yes No Select & Press ENTER
Figure 185
Meter being Reset Please wait.
Figure 186
Figure 187
11 ELECTRODE CARE
11.1 Electrode Activation
DO NOT touch or rub the glass bulb. If you follow the storage and maintenance procedure, you can use your electrode immediately. If the electrode responds sluggishly or drifts, the bulb may be dehydrated. Immerse the electrode in an ideal storage solution such as electrode storage solution or pH 4 buffer solution for 1-2 hours to hydrate it. See Storing pH/ORP electrodes below. If this procedure does not hydrate the electrode, reactivate or replace it. Use 2 or 3 point calibration to test your electrode performance. If you do not get good readings, use a different pH electrode to confirm the meter is working properly. If the results are still not satisfactory, consult your distributor/dealer.
12.2 Using with computer
Use OAKTON RS-232 cable 35615-09 to connect your meter to a computer. Refer to enclosed software disc for instructions on how to use software with your meter.
13 ADDITIONAL INFORMATION
13.1 pH and Temperature
The pH electrode is affected by temperature changes. Automatic Temperature Compensation (ATC) compensates for these temperature changes. Some solutions show an increase while others a decrease in pH with the same temperature change. Record the solution temperature along with the pH value, or the measurement may be meaningless. Temperature changes also affect the signal the pH electrode sends to the meter and causes a loss of accuracy for the reading. To limit the loss of accuracy during calibration, make the temperature of the pH buffer calibrating solutions and the sample solution the same.
13.2 pH Buffer Calibration Solution
You can use standard buffer solutions to calibrate a pH meter before you measure the pH of a sample. Calibration solutions serve as basis of comparison between measurements. The most common standard buffers are pH 4.01, pH 7.00 and pH 10.01. For 1-point calibration, use a standard buffer of pH 7.00 or 6.86, or a standard or custom buffer whose pH value is close to that of the sample. Use 2-point calibration when you know the sample is acidic (low pH) or basic (high pH). For example: in acidic samples, use standard buffers such as pH 7.00 and pH 4.01; in basic samples, use standards such as pH 7.00 and pH 10.01. Use multi-point calibration when the sample pH is completely unknown or for best accuracy over the entire pH range. Contact your distributor for information on pH buffer and calibration solutions.
13.3 Standard pH Buffers
The following table shows the various pH values at different temperature of the solution during calibration. The table also illustrates why a calibration value may be different from the buffer value at 25C. USA Buffer 1.105 1.67 1.67 1.67 1.67 1.68 1.68 1.69 1.69 1.70 1.70 1.71 1.72 1.73 1.73 1.74 1.75 1.77 1.78 1.80 1.81 1.81 1.81 4.01 4.01 4.01 4.01 4.00 4.00 4.01 4.01 4.02 4.03 4.04 4.06 4.08 4.10 4.11 4.12 4.14 4.16 4.18 4.23 4.23 4.23 4.23 7.00 7.12 7.09 7.06 7.04 7.02 7.00 6.99 6.98 6.97 6.97 6.97 6.97 6.98 6.98 6.99 6.99 7.00 7.01 7.02 7.03 7.03 7.03 10.01 10.32 10.25 10.18 10.12 10.06 10.01 9.97 9.93 9.93 9.86 9.83 9.81 9.79 9.77 9.76 9.75 9.74 9.73 9.73 9.74 9.74 9.74 12.45 13.43 13.21 13.00 12.81 12.63 12.45 12.29 12.13 11.99 11.84 11.70 11.58 11.45 11.45 11.45 11.45 11.45 11.45 11.45 11.45 11.45 11.45 1.68 1.67 1.67 1.67 1.67 1.68 1.68 1.69 1.69 1.70 1.70 1.71 1.72 1.73 1.73 1.74 1.75 1.77 1.78 1.80 1.81 1.81 1.81 4.01 4.01 4.01 4.01 4.00 4.00 4.01 4.01 4.02 4.03 4.04 4.06 4.08 4.10 4.11 4.12 4.14 4.16 4.18 4.23 4.23 4.23 4.23 NIST Buffer 6.86 6.98 6.95 6.92 6.90 6.87 6.86 6.85 6.84 6.84 6.83 6.83 6.83 6.84 6.84 6.84 6.85 6.86 6.87 6.88 6.88 6.88 6.88 9.18 9.46 9.40 9.33 9.28 9.23 9.18 9.14 9.11 9.07 9.04 9.01 8.99 8.96 8.94 8.92 8.91 8.89 8.87 8.85 8.85 8.85 8.85 12.45 13.43 13.21 13.00 12.81 12.63 12.45 12.29 12.13 11.99 11.84 11.70 11.58 11.45 11.45 11.45 11.45 11.45 11.45 11.45 11.45 11.45 11.45
Indicates
Memory write error Memory checksum error DTR line is disconnected Frame/parity errors Received buffer overflowing pH offset too much
Unit is too old (> 10 years) Hardware failure Hardware fault
Turn meter off and return to authorized distributor if necessary Turn meter off and return to authorized distributor if necessary Turn meter off and return to authorized distributor if necessary Turn meter off and return to authorized distributor if necessary Turn meter off and return to authorized distributor if necessary
pH offset should not exceed 1 pH from the display
Check electrode condition Make sure buffer is fresh and correct Recalibrate meter
Error: pH Slope Error
Incorrect pH slope
pH slope is out of allowable limit
Error: Ion Slope Error (pH 2100 meter only) Error: mV Offset too large Error: Out of Range Error: ATC offset too much Error: Too much offset@7pH Error: Slope out:75%-105% Error: Pts too close Or slope diff. sign
Incorrect ion slope
Average ion slope is not within 10mV-75mV/decade
Offset too much Out of Range Offset of temp. probe too much Offset too much
Value input is not within 150.0mV from the display Value input exceeds the specified range Temp. calibration offset is o o not within 5 C (or 9 F) pH offset should not exceed 1 pH from the display (custom pH buffer) pH slope is not within 75% to 105% (custom pH buffer) Slope is not negative or cal. Points are not 1 pH apart (custom pH buffer)
Recalibrate meter Re-enter value Re-enter value Re-enter value
Incorrect pH slope Incorrect slope alignment
Re-enter value Re-enter value
16 SPECIFICATIONS
pH Range Resolution Accuracy Calibration -1.000 to 14.000 pH 0.001 / 0.01 pH (user-selectable) 0.002 / 0.01 pH 1 to 5 points (standard buffers); first point must be pH 7.000, 6.860 (offset) Min. 2 points and Max. 5 points for custom entry 1 - USA: pH 1.68, 4.01, 7.00, 10.01, 12.45 2- NIST: pH 1.68, 4.01, 6.86, 9.18, 12.45 3- Bf1: pH 1.68, 4.01, 6.86, 10.01, 12.45 4- Bf2: pH 1.68, 4.01, 7.00, 9.18, 12.- Custom entry buffer calibration - 1850.0 to 1850.0 mV 0.1 mV 0.2 mV mV offset up to 150 mV -5.0 to 105.0 oC; 23.0 to 221.0 oF 0.1 oC / oF 0.3 oC / 0.5 oF Manual Temperature compensation: adjust from -0.5 to 105.0C/ 23.0 to 221.0F Automatic Temperature compensation (ATC) offset 5.0C/ 9.0F pH 2100 meter only Ion Range Resolution (High resolution mode: 500.0 mV) 0.001 to 19999 0.001: from 0.001 to 0.999 0.01: from 1.00 to 9.99 0.1: from 10.0 to 99.9 1: from 100 to 19999 0.001: from 0.001 to 0.099 0.01: from 0.10 to 0.99 0.1: from 1.0 to 9.9 1: from 10 to 19999 0.5% of full scale for monovalent ions 1% of full scale for divalent ions Calibration Minimum Average Slope Maximum Average Slope Inputs Output Recorder Output Power Requirements Display Dimensions (L x W x H) Weight 2 to 5 points, First point keyed in. the rest are selected using the keys 10 mV/ decade 75 mV/ decade BNC, Phono (ATC), Reference, Ground RS232C 1800 mV, 1 mV/mV unit AC/DC 9V Adapter (110 VAC/220 VAC) Custom Dual LCD (1 x 4 digit, 1 x 3.5 digit, 24 annunicators) 230 x 180 x 63 mm (meter only); 395 x 260 x 90 mm (boxed) 1.4lbs/ 850 gm (unit); 1400 gm (boxed) MI and MR
18 WARRANTY
Eutech Instruments/ Oakton Instruments supplies this bench meter with a 3-year warranty and 6-month warranty for against manufacturing defects from the date of purchase. If repair or adjustment is necessary and has not been the result of abuse or misuse within the warranty period, please return, freight prepaid, and correction will be made without charge. Out of warranty items will be repaired on a charge basis. Exclusions to the Warranty The warranty shall not apply to defects resulting from: Improper or inadequate maintenance by customer; Unauthorized modification or misuse; Operation outside of the environmental specifications of the products. Return of Items Authorization must be obtained from your Authorized Distributor or Customer Service Dept. before returning items for any reason. When applying for authorization, please include data regarding reason the items are to be returned. Packing the item for repair should be done using the original packaging or material, with information about any fault identified. Shipment damage as a result of inadequate packaging is your or your distributors responsibility, whoever applicable.
Eutech Instruments/ Oakton Instruments reserves the rights to make improvements in design, construction, and appearance of products without notice.
For more information on Eutech Instruments/ Oakton Instruments products, contact your nearest distributor or visit our website listed below:
Oakton Instruments P.O Box 5136, Vernon Hills, IL60061, USA Fax: (1) 847-247-2984 www.4oakton.com www.oaktoninstruments.com
Eutech Instruments Pte Ltd Blk 55, Ayer Rajah Crescent, #04-16/24 Singapore 139949 Tel: (65) Fax: (65) E-mail: marketing@eutechinst.com Web-site: www.eutechinst.com
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